Part 1 Basic Knowledge in Organic Chemistry Laboratory
1.1 Rules in laboratory
1.2 Prevention and treatment of the common accidents in laboratory
1.3 Requirements of preparation, record and report of experiments
1.4 Common lab equipment and apparatus
1.5 Waste disposal
1.6 Notes for organic synthesis devices and safety
1.7 Names of important organic compounds
Part 2 Basic Experimental Techniques
2.1 Preparation of organic compounds
2.2 The determination of physical constants of organic compounds
2.3 Separation and purification technology of organic compounds
2.4 Spectral analysis technology of organic compounds
Part 3 Experiments for Preparation of Organic Compounds
3.1 Preparation of cyclohexene
3.2 Preparation of anhydrous ethanol
3.3 Preparation of n-butyl bromide
3.4 Preparation of n-butyl ether
3.5 Preparation of acetophenone
3.6 Preparation of aspirin
3.7 Preparation of cinnamic acid
3.8 Preparanon of n-butyl acetate
3.9 Preparation of isoamyl acetate
3.10 Synthesis of glycerol monostearate
3.11 Preparation of skin care cosmetic
3.12 Preparation of detergent
3.13 Design an experiment procedure for the synthesis of ethyl acetate
3.14 Design an experiment procedure for the purification of N-phenylacetamide
Part 4 Extraction, Separation and Identification of Organic Compounds
4.1 Distilling 95% ethanol and measuring the boiling point
4.2 Recrystallization of benzoic acid
4.3 Purification of benzaldehyde
4.4 Isolation of caffeine from tea leaves
4.5 The extraction of limonene from orange peels
4.6 Separation of A and B by thin-layer chromatography
4.7 Separation of spinach pigments by column chromatography
4.8 Preparation and resolution for optical isomers of tris(ethylenediamine) cobalt salts
4.9 Identification of sugar
4.10 Identification of amino acids and proteins
4.11 Design an experiment procedure for the purification of ethanol
4.12 Design an experimental procedure for the identification of caffeine by thin-layer chromatography
4.13 Design an experimental procedure for the extraction of pigments from natural product
Part 5 Experimental Diagram
5.1 Distilling 95% ethanol and measuring the boiling point
5.2 Isolation of caffeine from tea leaves and sublimation
5.3 Synthesis, isolation and purification of n-butyl acetate
5.4 Separation of mixture and identification by thin-layer chromatography
5.5 Preparation of aspirin
5.6 R.ecrystallization of benzoic acid
5.7 The preparation of n-butyl bromide
5.8 The synthesis of n-butyl ether
Part 6 有機(jī)化學(xué)實(shí)驗(yàn)室和設(shè)備安全常識(shí)
6.1 有機(jī)化學(xué)實(shí)驗(yàn)室安全知識(shí)
6.2 有機(jī)合成常用設(shè)備使用常識(shí)
References
Appendix
I. Physical constant
II. Name of glassware